Benzoyl chloride → HCID 70378238, compound
Reaction equation
[CH3:1][C:2]1[CH:10]=[C:9]2[C:5]([C:6]([CH2:11][CH2:12][N:13]3[CH2:18][CH2:17][NH:16][CH:15]([CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])[C:14]3=[O:25])=[CH:7][NH:8]2)=[CH:4][CH:3]=1.[C:26](Cl)(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:26]([N:16]1[CH2:17][CH2:18][N:13]([CH2:12][CH2:11][C:6]2[C:5]3[C:9](=[CH:10][C:2]([CH3:1])=[CH:3][CH:4]=3)[NH:8][CH:7]=2)[C:14](=[O:25])[CH:15]1[CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1Participants
3
Procedure
Using the procedure of Step D of Example 1, 10 g of the product of Step C and 3.36 ml of benzoyl chloride were reacted to obtain 13 g of expected product melting at 155° C.
Workup
- customwere reacted
Sources & evidence
- ORD record
- ord-f314f8fe59cb44abbe1e56a07000661c
- Source dataset
- uspto-grants-1989_12
- Patent number
- US04886802
Reaction notes
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