Benzoyl chloride → HCID 70378213, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][CH:6]=[C:5]2[CH2:11][CH2:12][N:13]1[CH2:18][CH2:17][NH:16][CH:15]([CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])[C:14]1=[O:25].[C:26](Cl)(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:26]([N:16]1[CH2:17][CH2:18][N:13]([CH2:12][CH2:11][C:5]2[C:4]3[C:8](=[CH:9][CH:10]=[C:2]([Cl:1])[CH:3]=3)[NH:7][CH:6]=2)[C:14](=[O:25])[CH:15]1[CH2:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1Participants
3
Procedure
Using the procedure of Step D of Example 1, 11 g of the product of Step C and 3.5 ml of benzoyl chloride were reacted to obtain 13 g of the expected product.
Workup
- customwere reacted
Sources & evidence
- ORD record
- ord-b3cc462bc0254fa18865aa42e29473cc
- Source dataset
- uspto-grants-1989_12
- Patent number
- US04886802
Reaction notes
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