HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 14698771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 3-Benzyl-5-(hydroxymethyl)-1,3-oxazolidin-2-one | HCID 2793798 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 14698771 | HCID 14698771 | 81% |
Reaction Steps
A solution of 20 g (0.1 mole) of 3-benzyl-5-hydroxymethyl-2-oxazolidinone and 24 g (0.2 mole) of sulfonyl chloride in chloroform was refluxed for 3 hr. The reaction mixture was dried over anhydrous sodium sulfate, concentrated and subjected to distillation to give 18.2 g (81%) liquid, b.p. 176°-178° C. at 0.1 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886794 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-82f85d06cbf148ff8835d9cb30cd827d |
| Source note | uspto-grants-1989_12 |