HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Salicylate → 3-Hydroxy-2,2-bis(hydroxymethyl)propyl 2-hydroxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Salicylate | HCID 4133 | — |
| Reactant | Pentaerythritol | HCID 8285 | — |
| Reactant | 2,3-Dihydroxypropyl salicylate | HCID 3849318 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Product | 3-Hydroxy-2,2-bis(hydroxymethyl)propyl 2-hydroxybenzoate | HCID 19837326 | — |
Reaction Steps
Pentaerythritol salicylate was prepared by the method described in Example 1 for the preparation of glycerol salicylate except that the reactants were pentaerythritol (34.04 g; 0.25 moles), methyl salicylate (86.72 g; 0.57 moles) and sodium methoxide (0.41 g; 0.0075 moles). The final methyl salicylate level was 12.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886843 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-929740d7afbb49628dcd4ca281163c70 |
| Source note | uspto-grants-1989_12 |