HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(2-aminoethyl)benzoate → HCID 14076217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(2-aminoethyl)benzoate | HCID 12945884 | — |
| Reactant | HCID 21667689 | HCID 21667689 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 14076217 | HCID 14076217 | — |
Reaction Steps
Prepared analogously to Example 3 by reaction of 2-(4-carboethoxyphenyl)ethylamine and stoichiometric amounts of triethylamine with 2-benzoylamino-4-methyl-5-bromoacetyl-thiazole, followed by reduction and purification of the base on a silica gel column using chloroform/methanol=9:1 as eluant and trituration with petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886814 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-456ec178cf6b4e0183c307f7fbf0ba44 |
| Source note | uspto-grants-1989_12 |