HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → Ethyl (3-benzoylphenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | (3-Benzoylphenyl)acetic acid | HCID 30931 | — |
| Reactant | Ethyl (3-phenoxyphenyl)acetate | HCID 12509092 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl (3-benzoylphenyl)acetate | HCID 53948061 | — |
Reaction Steps
The procedure is as in Example 33 for the preparation of ethyl (3-phenoxyphenyl)acetate, starting with (3-benzoylphenyl)acetic acid (16.6 g) and 36N aqueous sulphuric acid solution (2 cc) in ethanol (200 cc). Ethyl (3-benzoylphenyl)acetate (16.8 g) is obtained in the form of a brown oil, and is used in the crude state in the subsequent syntheses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04886835 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-2b67ce1645fc45bd92e8a754433b1f36 |
| Source note | uspto-grants-1989_12 |