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HRID477602

反应详情

EQUATION

反应方程式

HRID 477602 的结构方程式

REACTANTS

反应物

2
结构：NCCO
HCID700

Ethanolamine

C2H7NO

结构：O=[N+]([O-])c1cc2c(c([N+](=O)[O-])c1)OCC2
HCID19836322

5,7-Dinitro-2,3-dihydro-1-benzofuran

C8H6N2O5

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cc(CCO)c(NCCO)c([N+](=O)[O-])c1
HCID19836337

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

0.29 Mole (60.9 g) of 2,3-dihydro-5,7-dinitrobenzofuran is added in small portions at room temperature to 122 ml of 2-aminoethanol. After the addition is complete, the reaction medium is brought for 15 minutes to 95° C. 500 ml of water are added; after the mixture is cooled, the expected product is drained, and this, after being made into a paste in water and recrystallized from 75 ml of 96° strength ethanol, melts at 115° C.

WORKUP

后处理

  1. additionAfter the addition
  2. temperatureafter the mixture is cooled