HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 15105970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Dibenzylhydroxylamine | HCID 69297 | — |
| Reactant | HCID 15135146 | HCID 15135146 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 15105970 | HCID 15105970 | 11.6% |
Reaction Steps
The compound is prepared using the method of Example II, with 16.20 g of 3-(3,5-di-tert-butyl-4-hydroxybenzylthio)propanoic acid, 10.66 g of N,N-dibenzylhydroxylamine, 5.06 g of triethylamine, and 6.35 g of oxalyl chloride. The residue is purified by preparative HPLC to give 3.0 g of a white solid: mp 84°-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04888444 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-bebd28dc86424242a536f6a3d61aa0d4 |
| Source note | uspto-grants-1989_12 |