HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 477741Generated: October 29, 2026
2,6-Dichloroaniline → HCID 19872285, compound
https://huagongshe.com/reaction/477741
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2,6-Dichloroaniline | HCID 11846 | — |
| Reactant | 1-Acetyl-5-amino-1H-1,2,4-triazole-3-sulfonyl chloride | HCID 14255123 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19872285 | HCID 19872285 | 94.7% |
Reaction Steps
The product of stage (c) (54 g) was treated with 2,6-dichloroaniline (42.63 g) in pyridine (350 ml), and the mixture was stirred at 60° C. for 12 hours. After cooling, the product was filtered off, washed with a little pyridine and ether, and dried in vacuo to give 53.6 g of the desired product, mp 213°-215° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04889553 |
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| Source dataset | uspto-grants-1989_12 |
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| ORD ID | ord-1b9426869b8747bd9e7f4dadbef2f1f4 |
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| Source note | uspto-grants-1989_12 |
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