HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 477750Generated: October 25, 2026
Hydrochloric Acid → HCID 178518561, compound
https://huagongshe.com/reaction/477750
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1-Ethoxycarbonyl-1-phenythiosemicarbazide | HCID 85773191 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178518561 | HCID 178518561 | 86.6% |
Reaction Steps
The product of stage (a) (28.9 g) was treated with a solution of sodium hydroxide (7.5 g) in water (150 ml). The suspension was heated under reflux with stirring for 45 minutes and then cooled to 25° C. The pH of the solution was adjusted to 1.0 with concentrated hydrochloric acid and the resulting solid was filtered and washed with water to give 20.2 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04889553 |
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| Source dataset | uspto-grants-1989_12 |
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| ORD ID | ord-d83609b28ff9451b83aa088a0179c252 |
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| Source note | uspto-grants-1989_12 |
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