Morpholine → 122910-82-1

HRID 477819Notes

Reaction equation

HRID 477819 reaction equation
[Cl:1]C[CH:3]1[O:8][CH2:7][CH2:6][N:5]([CH2:9][C:10]2[CH:15]=CC=CC=2)[CH2:4]1.[NH:16]1CC[O:19][CH2:18][CH2:17]1>>[ClH:1].[ClH:1].[O:8]1[CH2:3][CH2:4][N:5]([CH2:9][CH:10]2[O:19][CH2:18][CH2:17][NH:16][CH2:15]2)[CH2:6][CH2:7]1

Participants

3

Reactant 2

HCID 8083MorpholineHCID 28015624-Benzyl-2-(chloromethyl)morpholine

Product 1

HCID 14627571122910-82-1

Procedure

By the use of 2-chloromethyl-4-benzylmorpholine and morpholine, the reaction is similarly carried out as Reference example 2 to give 2-(morpholinomethyl)morpholine dihydrochloride as white crystals, melting at 297°-299° C. with decompostion.

Sources & evidence

ORD record
ord-b9a4b49dbb604bc0ba9e373215b34b1d
Source dataset
uspto-grants-1989_12
Patent number
US04889857

Reaction notes

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