HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 13649442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 13649441 | HCID 13649441 | — |
| Product | HCID 13649442 | HCID 13649442 | — |
Reaction Steps
A solution of 0.76 g 6-aminomethyl-2-(p-ethoxycarbonylphenyl)pyridine in 10 ml of formic acid is heated at 90° for 15 h. The reaction mixture is cooled to 0°, made basic with excess saturated ammonium hydroxide solution and extracted with chloroform. The organic extracts are dried and evaporated to yield the title compound (c) which is recrystallized from toluene, m.p. 119.5°-120.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04889861 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-c530748d658a44c0894db2878d255189 |
| Source note | uspto-grants-1989_12 |