HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbonic Acid → 1-Methyl-4,6,7,8-tetrahydro-2(3H)-naphthalenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbonic Acid | HCID 767 | — |
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | Carvone, (+-)- | HCID 7439 | — |
| Reactant | Cyclohexanone, 2-hydroxy- | HCID 10785 | — |
| Product | 1-Methyl-4,6,7,8-tetrahydro-2(3H)-naphthalenone | HCID 19835392 | — |
Reaction Steps
This material is prepared according to the procedure for Preparation 6 wherein 2-hydroxycyclohexanone is substituted for carvone. The resulting hydroxyketone is converted to the semicarbazone before dehydration with aqueous oxalic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04889947 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-4ec6c56119a54402927d9d281f967d94 |
| Source note | uspto-grants-1989_12 |