HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 14877744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14877743 | HCID 14877743 | — |
| Catalyst | Hexadecyltrimethylammonium chloride | HCID 8154 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 14877744 | HCID 14877744 | 89% |
Reaction Steps
18.6 g (30 millimole) of 1-O-tetradecyl-3-O-[2-(2-trityloxyethoxy)ethyl]glycerol, 6.1 g (33 millimole) of methyl p-toluenesulfonate, 8 g (100 millimole) of 50% sodium hydroxide, 192 mg (0.6 millimole) of cetyltrimethylammonium chloride and 20 ml of 2N hydrochloric acid were treated by following a procedure similar to that of Working Example 5, to give 10.4 g (89%) of the above-captioned compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04889953 |
| Source dataset | uspto-grants-1989_12 |
| ORD ID | ord-2e4f31a9e82943238a5d54ecf119d172 |
| Source note | uspto-grants-1989_12 |