HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 18001180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 18001152 | HCID 18001152 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 18001180 | HCID 18001180 | — |
Reaction Steps
The title compound, MS: m/e=578.1 (M+H+), [α]58920=−19.14 (c=0.4545, chloroform), was prepared in accordance with the general method of example 102 (part1) and example 38 from (−)-(1-{4-[1-(3,5-bis-trifluoromethyl-benzoyl)-3-p-tolyl-piperidin-4-yl]-piperazin-1-yl}-2,2,2-trifluoro-ethanone and methane sulfonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642226B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-8cb7dac611cb49eabbe22889b3bf93db |
| Source note | uspto-grants-2003_11 |