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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 478440Generated: October 30, 2026

Methanesulfonyl chloride → HCID 18001180, compound

https://huagongshe.com/reaction/478440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonyl chlorideHCID 31297—
ReactantHCID 18001152HCID 18001152—
SolventChloroformHCID 6212—
ProductHCID 18001180HCID 18001180—

Reaction Steps

The title compound, MS: m/e=578.1 (M+H+), [α]58920=−19.14 (c=0.4545, chloroform), was prepared in accordance with the general method of example 102 (part1) and example 38 from (−)-(1-{4-[1-(3,5-bis-trifluoromethyl-benzoyl)-3-p-tolyl-piperidin-4-yl]-piperazin-1-yl}-2,2,2-trifluoro-ethanone and methane sulfonyl chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06642226B2
Source datasetuspto-grants-2003_11
ORD IDord-8cb7dac611cb49eabbe22889b3bf93db
Source noteuspto-grants-2003_11