HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromomethylcyclopropane → HCID 9851092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | HCID 10211148 | HCID 10211148 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 9851092 | HCID 9851092 | — |
Reaction Steps
The title compound, MS: m/e=574.1 (M+H+), [α]58920=−18.46, [α]54620=−27.04, (c=0.3846, chloroform), was prepared in accordance with the general method of example 102 from (−)-1-{4-[1-(3,5-bis-trifluoromethyl-benzoyl)-3-(4-chloro-phenyl)-piperidin-4-yl]-piperazin-1-yl}-2,2,2-trifluoro-ethanone and cyclopropylmethylbromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642226B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-8c414d513a0b46dd9082386c673d56c2 |
| Source note | uspto-grants-2003_11 |