HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22064513, compound → 498546-32-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22064513 | HCID 22064513 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 498546-32-0 | HCID 22064531 | — |
Reaction Steps
A solution of 1 g of the compound obtained in Step 1 in 18 ml of hydrochloric acid is refluxed for 4 hours and then poured onto ice. The precipitate formed is filtered off, washed with water until the pH is 5-6 and then dried, allowing the expected product to be isolated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642248B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-087c1d3dd4404494aaac4f4b2d48a6b6 |
| Source note | uspto-grants-2003_11 |