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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 478809Generated: October 29, 2026

Isobutanol → HCID 15481774, compound

https://huagongshe.com/reaction/478809

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsobutanolHCID 6560—
ReactantN-Phenylacetyl-L-leucineHCID 11983894—
SolventChloroformHCID 6212—
ProductHCID 15481774HCID 15481774—

Reaction Steps

N-Phenylacetyl-L-leucine (0.0081 g, 0.038 mmol) was dissolved in 2.0 mL CHCl3 (EtOH free) and iso-butyl alcohol (0.055 mL) and treated with P-EPC (100 mg, 0.87 milliequivalents). The mixture was rotated for 4 days, filtered through a plug of cotton and the filtrate evaporated at reduced pressure to an oil which was sufficiently pure for testing.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06642261B2
Source datasetuspto-grants-2003_11
ORD IDord-bc79a6879c184d0eafc047f5474a3de5
Source noteuspto-grants-2003_11