Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(1-Methylcyclopropyl)methanol → N-[(3-chlorophenyl)acetyl]alanine (1-methylcyclopropyl)methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (1-Methylcyclopropyl)methanol | HCID 137701 | — |
| 반응물 | N-(3-chlorophenylacetyl)alanine | HCID 15481783 | — |
| 생성물 | N-[(3-chlorophenyl)acetyl]alanine (1-methylcyclopropyl)methyl ester | HCID 20613258 | — |
반응 단계
Following General Procedure C above, and using N-(3-chloroph,enylacetyl alanine (from Example D above) and (1-methylcyclopropyl)methanol (Aldrich) the title compound can be prepared. The reaction was monitored by tlc on silica gel and purification was by liquid chromatography using 3:7 EtOAc:hexane as the eluant. NMR data was as follows:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06642261B2 |
| 출처 데이터셋 | uspto-grants-2003_11 |
| ORD ID | ord-14b0b2b745cf44b5a0df36d09dae0af5 |
| 출처 메모 | uspto-grants-2003_11 |