HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexen-1-OL → HCID 15481775, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexen-1-OL | HCID 13198 | — |
| Reactant | N-(3-chlorophenylacetyl)alanine | HCID 15481783 | — |
| Product | HCID 15481775 | HCID 15481775 | — |
Reaction Steps
Following General Procedure C above, and using N-(3-chlorophenylacetyl alanine (from Example D above) and cyclohex-2-en-1-ol (Aldrich) the title compound can be prepared. The reaction was monitored by tlc on silica gel and purification was by liquid chromatography using 3:7 EtOAc:hexane as the eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642261B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-729a5a41cbda4f10b04121578e4199e8 |
| Source note | uspto-grants-2003_11 |