HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
m-Tolylacetic acid → N-[(3-methylphenyl)acetyl]alanine Iso-butyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | m-Tolylacetic acid | HCID 12121 | — |
| Edukt | 2-methylpropyl (2S)-2-aminopropanoate | HCID 13743556 | — |
| Produkt | N-[(3-methylphenyl)acetyl]alanine Iso-butyl Ester | HCID 53803690 | — |
Reaktionsschritte
Following General Procedure I above, and using 3-methylphenylacetic acid (Aldrich) and alanine iso-butyl ester (prepared following General Procedure J above), the title compound was prepared. The reaction was monitored by tl c on silica gel and purification was by filtration as described in the general procedure. NMR data was as follows:
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06642261B2 |
| Quelldatensatz | uspto-grants-2003_11 |
| ORD ID | ord-0e35700013c347b3b661b2e7e62e649f |
| Quellennotiz | uspto-grants-2003_11 |