HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenylacetic acid → N-[(3-nitrophenyl)acetyl]methionine Ethyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenylacetic acid | HCID 15876 | — |
| Reactant | Ethyl L-methionate hydrochloride | HCID 3083785 | — |
| Product | N-[(3-nitrophenyl)acetyl]methionine Ethyl Ester | HCID 53910855 | — |
Reaction Steps
Following General Procedure G above and using 3-nitrophenylacetic acid (Aldrich) and methionine ethyl ester hydrochloride (Aldrich), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by recrystallization from butyl chloride. NMR data was as follows:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642261B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-abe2b7fdc7cb4a2d90b9a56ab0d67f7b |
| Source note | uspto-grants-2003_11 |