HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → 6-(2-azidoethanoyl)-3H-benzothiazol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 6-(Chloroacetyl)-1,3-benzothiazol-2(3H)-one | HCID 14116707 | — |
| Product | 6-(2-azidoethanoyl)-3H-benzothiazol-2-one | HCID 18002782 | 96% |
Reaction Steps
Treatment of 6-(2-chloroethanoyl)-3H-benzothiazol-2-one with sodium azide, following the procedure described in Example 6, Step 4, gave 6-(2-azidoethanoyl)-3H-benzothiazol-2-one (6.95 g, 96%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642256B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-3f2f80d82c034e1cb65808ac0ec61359 |
| Source note | uspto-grants-2003_11 |