HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → 5-(2-Azidoacetyl)-1,3-dihydro-2H-benzimidazol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | 5-(2-Chloro-acetyl)-1,3-dihydro-benzoimidazol-2-one | HCID 2402659 | — |
| Product | 5-(2-Azidoacetyl)-1,3-dihydro-2H-benzimidazol-2-one | HCID 18002808 | 93% |
Reaction Steps
Treatment of give 5-(2-chloroethanoyl)-1,3-dihydrobenzimidazol-2-one with sodium azide, following the procedure described in Example 6. Step 4, gave 6-(2-azidoethanoyl)-1,3-dihydrobenzimidazol-2-one (5.75 g, 93%):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642256B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-d789a114ef5c4e2eb771c17a877bae19 |
| Source note | uspto-grants-2003_11 |