HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → 8-ethyl-8-tricyclo[5.2.1.02,6]decanyl-5-norbornene-2-carboxylate maleic Anhydride cis-5-norbornene-endo-2,3-dicarboxylic Anhydride acrylic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | Maleic Anhydride | HCID 7923 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | cis-5-Norbornene-endo-2,3-dicarboxylic anhydride | HCID 9964188 | — |
| Reactant | 8-Ethyl-8-tricyclo[5.2.1.02,6]decanyl-5-norbornene-2-carboxylate | HCID 18003142 | — |
| Product | 8-ethyl-8-tricyclo[5.2.1.02,6]decanyl-5-norbornene-2-carboxylate maleic Anhydride cis-5-norbornene-endo-2,3-dicarboxylic Anhydride acrylic Acid | HCID 131724200 | — |
Reaction Steps
80 mmol of 8-ethyl-8-tricyclo[5.2.1.02,6]decanyl-5-norbornene-2-carboxylate, 100 mmol of maleic anhydride, 15 mmol of cis-5-norbornene-endo-2,3-dicarboxylic anhydride and 5 mmol of acrylic acid were dissolved in 1 equivalent of anhydrous ethyl acetate, and then polymerization and separation were carried out in the same manner as in Example 18, to separate 4.56 g of a polymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642336B1 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-b304e64402004b709ee8266b9389f0be |
| Source note | uspto-grants-2003_11 |