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Ethanol → sodium 2-(4-(N-salicyloyl)aminophenyl)propionate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 2-(4-(N-salicyloyl)aminophenyl)propionic acid | HCID 9817303 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | sodium 2-(4-(N-salicyloyl)aminophenyl)propionate | HCID 23700501 | 92.1% |
反応手順
A solution of 53.05 g (0.186 mol) of 2-(4-(N-salicyloyl)aminophenyl)propionic acid and 300 ml of ethanol was treated with 7.59 g (0.190 mol) of NaOH dissolved in 22 ml of water. The reaction mixture was stirred for 30 min at 25C. and for 30 min at 0° C. The resulting pale yellow solid was isolated by filtration to give 52.61 g of sodium 2-(4-(N-salicyloyl)aminophenyl)propionate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06642411B1 |
| 出典データセット | uspto-grants-2003_11 |
| ORD ID | ord-5e9711d0561f492aadde069ec7874bd6 |
| 出典メモ | uspto-grants-2003_11 |