HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzyl mercaptan → (Z)-2,4,6-trifluorostyryl4-methylbenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzyl mercaptan | HCID 78252 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2-Ethynyl-1,3,5-trifluorobenzene | HCID 18003771 | — |
| Product | (Z)-2,4,6-trifluorostyryl4-methylbenzylsulfide | HCID 86585664 | — |
Reaction Steps
A solution of 2,4,6-trifluorophenylacetylene (0.02 mol), 4-methylbenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to General Procedure 2 to form (Z)-2,4,6-trifluorostyryl-4-methylbenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to General Procedure 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642410B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-e02be16bd1de455294ed0f8865ffa58c |
| Source note | uspto-grants-2003_11 |