HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → (Z)-3,4-dihydroxystyryl-2,4,6-trimethoxybenzylsulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | (2,4,6-Trimethoxyphenyl)methanethiol | HCID 10608677 | — |
| Reactant | 4-Ethynylbenzene-1,2-diol | HCID 22603778 | — |
| Product | (Z)-3,4-dihydroxystyryl-2,4,6-trimethoxybenzylsulfide | HCID 86585666 | — |
Reaction Steps
A solution of 3,4-dihydroxyphenylacetylene (0.02 mol), 2,4,6-trimethoxybenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to General Procedure 2 to form (Z)-3,4-dihydroxystyryl-2,4,6-trimethoxybenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to General Procedure 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06642410B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-d2517bff452346829111f3c024c500df |
| Source note | uspto-grants-2003_11 |