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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 479022Generated: October 25, 2026

4-Nitrobenzyl mercaptan → HCID 86585667, compound

https://huagongshe.com/reaction/479022

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Nitrobenzyl mercaptanHCID 193619—
ReactantSodiumHCID 5360545—
Reactant2-Ethynyl-1,3,5-trifluorobenzeneHCID 18003771—
ProductHCID 86585667HCID 86585667—

Reaction Steps

A solution of 2,4,6-trifluorophenylacetylene (0.02 mol), 4-nitrobenzyl mercaptan (0.02 mol) and metallic sodium (0.02 g atom) is subjected to General Procedure 2 to form (Z)-2,4,6-trifluorostyryl-4-nitrobenzylsulfide. The title compound is obtained following oxidation of the sulfide, according to General Procedure 2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06642410B2
Source datasetuspto-grants-2003_11
ORD IDord-e102226ed6e74443813c20b64faaabe1
Source noteuspto-grants-2003_11