HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 57156543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 20599271 | HCID 20599271 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57156543 | HCID 57156543 | 63.3% |
Reaction Steps
Silyl deprotection of 3β-hydroxy-4,4-dimethyl-(25R)-26-(tert-butyldimethylsilyloxy)cholest-5-ene (60 mg, 0.11 mmol) with tetrabutyl ammonium fluoride and recrystallisation from methanol to give 4,4-dimethyl-(25R)-cholest-5-ene-3β,26-diol (30 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06645953B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-32efab3bcf05426b9f72c40a284842cd |
| Source note | uspto-grants-2003_11 |