Dimethyl Sulfate → HCID 18770476, compound

Participants

Reaction Conditions

Reaction Steps

300 cm3 of nitrobenzene are introduced into a 1-dm3 three-necked flask and then 11.2 g (0.0446 mol) of 2-acetamido-9-aminoacridine and 11 cm3 (0.116 mol) of dimethyl sulphate are successively introduced, with stirring. The mixture is then heated at 140° C. for 20 minutes. After cooling, the precipitate obtained is filtered, washed with 20 cm3 of nitrobenzene and six times 20 cm3 of diethyl ether, air-dried and 14.35 g (85%) of 2-acetamido-9-amino-10-methylacridinium sulphate are obtained.

Provenance & Evidence