Nitric Acid → HCID 18770512, compound

HRID 479328Notes

Reaction equation

HRID 479328 reaction equation
[N+:1]([O-:4])([OH:3])=[O:2].[CH2:5]1[CH2:10][CH2:9][CH:8]([CH:11]([CH:19]2[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]2)[CH2:12][CH:13]2[NH:18][CH2:17][CH2:16][CH2:15][CH2:14]2)[CH2:7][CH2:6]1>C(#N)C.CO>[CH2:5]1[CH2:6][CH2:7][CH:8]([CH:11]([CH:19]2[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]2)[CH2:12][CH:13]2[NH:18][CH2:17][CH2:16][CH2:15][CH2:14]2)[CH2:9][CH2:10]1.[N+:1]([O-:4])([O-:3])=[O:2]

Participants

5

Reactant 2

HCID 944Nitric AcidHCID 4746Perhexiline

Product 1

HCID 18770512HCID 18770512, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 6342AcetonitrileSolvent

Conditions

Temperature
0 °C

Procedure

Nitric acid 65% (0.75 ml) is added to a Perhexiline solution (3.02 g, 10.9 mmole) in acetonitrile and methanol (10 ml), cooled at 0° C.

Sources & evidence

ORD record
ord-ac25a01204e741a09f62d814c5cddfef
Source dataset
uspto-grants-2003_11
Patent number
US06645965B1

Reaction notes

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