Hydrochloric Acid → HCID 18770414, compound

Participants

Reaction Steps

Concentrated hydrochloric acid (0.030 ml; 0.36 mmol) was added to a solution of N,N′-bis[1-[4-(3,4,5-trimethoxyphenyl)benzoyl]-4-piperidinyl]-N,N′-dimethylethylenediamine (60 mg; 0.076 mmol) in ethanol (5 ml) and the reaction mixture was concentrated under reduced pressure. The concentrated residue was suspended in diethyl ether and collected by filtration to obtain the title compound as a colorless crystalline powder.

Provenance & Evidence