HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → N-[1-(1H-1,2,3-benzotriazol-1-yl)-2-(2,6,6-trimethyl-1-cyclohexen-1-yl)ethyl]-4-chlorobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 4-Chlorobenzamide | HCID 12084 | — |
| Reactant | beta-HOMOCYCLOCITRAL | HCID 61124 | — |
| Reactant | HCID 178418385 | HCID 178418385 | — |
| Product | N-[1-(1H-1,2,3-benzotriazol-1-yl)-2-(2,6,6-trimethyl-1-cyclohexen-1-yl)ethyl]-4-chlorobenzamide | HCID 18770613 | — |
Reaction Steps
Benzotriazole, 4-chlorobenzamide, (2,6,6-trimethyl-1-cyclohexenyl)acetaldehyde, and p-toluenesulfonic acid were processed as in Example 53A to provide the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06645968B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-fc414f74b04d404683097d62eec7f13d |
| Source note | uspto-grants-2003_11 |