HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon tetrabromide → 5-(Benzyloxy)-6-but-3-enylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon tetrabromide | HCID 11205 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | [5-(Benzyloxy)quinolin-6-yl]methanol | HCID 23431816 | — |
| Reactant | HCID 178455850 | HCID 178455850 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 5-(Benzyloxy)-6-but-3-enylquinoline | HCID 23431827 | — |
Reaction Steps
Treatment of [5-(benzyloxy)quinolin-6-yl]methanol with carbontetrabromide and triphenylphosphine in dichloromethane and subsequent treatment with allyl magnesiumbromide in tetrahydrofu ran following the procedure described for Example 1, step 1 provides 5-(benzyloxy)-6-but-3-enylquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06700001B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-3601a4ff3252475bba70f33fa073f404 |
| Source note | uspto-grants-2004_03 |