HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylpiperidine → HCID 18771946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylpiperidine | HCID 7974 | — |
| Reactant | 6-Bromopyridine-2-carbaldehyde | HCID 2757009 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18771946 | HCID 18771946 | — |
Reaction Steps
6] To 6-bromo-2-pyridinecarboxaldehyde (400 mg, 2.15 mmol) was added 2-methylpiperidine (0.4 mL, 3.22 mmol) in dry CH2Cl2 (10 mL) to give 2-bromo-6-[(2-methylpiperidinyl)methyl]pyridine as a pale yellow solid. MS m/z: 269.1(M+H). Calc'd for C12H17BrN2: 269.18.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06645990B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-a6546d0958114bdbb0e38eda7ca4080c |
| Source note | uspto-grants-2003_11 |