HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18772033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 18771777 | HCID 18771777 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18772033 | HCID 18772033 | — |
Reaction Steps
HCl (0.12 mL, 0.12 mmol, 1.0 M soln in Et2O) was added to ethyl 1-[6-[3-(2-(pyridin-4-yl)thiazol-4-yl)ureido]-pyridin-2-ylmethyl]piperidine-2-carboxylate (50 mg, 0.11 mmol, Example 74) in a solution of MeOH (2 mL) to give a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06645990B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-7d3f9ede9b234944a1bf40d5d22cbc0b |
| Source note | uspto-grants-2003_11 |