HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18771577, compound → HCID 20599300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18771577 | HCID 18771577 | — |
| Solvent | Ethanol hexane | HCID 21879635 | — |
| Product | HCID 20599300 | HCID 20599300 | — |
Reaction Steps
1-[6-(3-Methyl-piperidin-1-ylmethyl)-pyridin-2-yl]-3-(2-pyridin-4-yl-thiazol-4-yl)-urea (50 mg, 0.12 mmol, Example 78) was separated by chiral HPLC (Chiraltech Chiralcel OJ 50×4.6 mm i.d.) using hexane/EtOH/DEA (90:10:0.2) to give a white solid. MS m/z: 409.3 (M+H). Calc'd for C21H24N6OS-408.52.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06645990B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-50efa9eed331402fb0c80a4cc1b7d22d |
| Source note | uspto-grants-2003_11 |