HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → (E)-4-chlorostyryl-N-3-chlorophenyl Sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | (E)-2-(4-chlorophenyl)ethene-1-sulfonyl chloride | HCID 5938154 | — |
| Product | (E)-4-chlorostyryl-N-3-chlorophenyl Sulfonamide | HCID 10131451 | 31.8% |
Reaction Steps
A solution of (E)-4-chlorostyrylsulfonyl chloride (10 mmol) and 3-chloroaniline (10 mmol) was subjected to General Procedure 1, part B. The title compound, melting point 118-120° C., was obtained in 31.8% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06646009B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-b107d3f0dc2d4112831083b3eefe59d9 |
| Source note | uspto-grants-2003_11 |