4-Fluoroaniline → HCID 9857738, compound

HRID 479723Notes

Reaction equation

HRID 479723 reaction equation
[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9](Cl)(=[O:11])=[O:10])=[CH:5][CH:4]=1.[F:15][C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1>>[CH3:1][O:2][C:3]1[CH:14]=[CH:13][C:6](/[CH:7]=[CH:8]/[S:9]([NH:20][C:19]2[CH:21]=[CH:22][C:16]([F:15])=[CH:17][CH:18]=2)(=[O:11])=[O:10])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 97314-FluoroanilineHCID 12114473HCID 12114473, compound

Product 1

HCID 9857738HCID 9857738, compoundYield 60.3%

Procedure

A solution of (E)-4-methoxystyrylsulfonyl chloride (10 mmol) and 4-fluoroaniline (10 mmol) was subjected to General Procedure 1, part B. The title compound was obtained in 60.3% yield.

Sources & evidence

ORD record
ord-a583ce2b0b8e433281955ce7c690cdee
Source dataset
uspto-grants-2003_11
Patent number
US06646009B2

Reaction notes

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