Azobisisobutyronitrile → HCID 178449903, compound

Participants

Reaction Steps

5 ml of styrene (43 millimole), 0.0177 g of TETRATEMPO (1.13×10−5 mol) and 3.3 g of AIBN (2×10−5 mol) are used with 7.3 mg of TEMPO (4.7×10−5 mol). The procedure followed is the same as in Example 1. After polymerizing for 5 hours, a polymer is obtained, the chromatogram of which exhibits only a single broad peak (PI=1.4) with a slight shoulder towards the high masses.

Provenance & Evidence