HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Benzyl-5-nitropyridin-2(1H)-imine → HCID 3629459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Benzyl-5-nitropyridin-2(1H)-imine | HCID 261542 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3629459 | HCID 3629459 | 100.2% |
Reaction Steps
A mixture of 2-benzylamino-5-nitropyridine (2.02 g) and 10% Pd/C (202 mg) in ethanol (20 mL) was placed in a Paar bottle and shaken under hydrogen (50 PSI) for 3 h. The mixture was filtered through Celite using dichloromethane and concentrated in vacuo to afford 1.76 g of 2-benzylamino-5-aminopyridine as a burgundy oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06646124B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-9dc445af79d44fdb8db264d630730898 |
| Source note | uspto-grants-2003_11 |