HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethanolamine → Benzimidazol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethanolamine | HCID 7618 | — |
| Reactant | C.I. Pigment Orange | HCID 25535 | — |
| Solvent | Water | HCID 962 | — |
| Product | Benzimidazol-2-one | HCID 162542 | — |
Reaction Steps
20 g of C.I. pigment orange 60 having an average primary particle diameter of 85 nm (in which the content as metal ions having a valence of at least 2 was 320 ppm), 1.6 g of the pigment derivative (a′) and 110 g of deionized water were mixed, triethanolamine was added so as to adjust pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a pigment dispersion. The obtained water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped to NO.2 filter paper, to show no bleedings of the pigment derivative.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06648954B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-b4b770af8ebb4c63b982a36c2212f9d1 |
| Source note | uspto-grants-2003_11 |