HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Benzimidazol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Pigment Yellow 151 | HCID 43525 | — |
| Reactant | Tartrazine | HCID 164825 | — |
| Solvent | Water | HCID 962 | — |
| Product | Benzimidazol-2-one | HCID 162542 | — |
Reaction Steps
20 g of C.I. pigment yellow 151 having an average primary particle diameter of 80 nm (in which the content of metal ions having a valence of at least 2 was 270 ppm), 4 g of a commercially available dye C.I. acid yellow 23 and 110 g of deionized water were mixed, aqueous ammonia was added so as to adjust the pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a water-based pigment dispersion. The obtained water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped to NO.2 filter paper, to show bleeding of the dye.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06648954B2 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-b33c872aa8884064be760c27d7029ce2 |
| Source note | uspto-grants-2003_11 |