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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 479899Generated: October 25, 2026

Ammonia → Quinacridone

https://huagongshe.com/reaction/479899

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
Reactant5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dioneHCID 70423—
ReactantHCID 178427422HCID 178427422—
SolventWaterHCID 962—
ProductQuinacridoneHCID 13976—

Reaction Steps

20 g of C.I. pigment red 122 having an average primary particle diameter of 90 nm (in which the content of metal ions having a valence of at least 2 was 450 ppm), 4 g of a commercially available dye C.I. acid red 249 and 110 g of deionized water were mixed, aqueous ammonia was added so as to adjust the pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a water-based pigment dispersion. The obtained water-based pigment dispersion had a high viscosity and caused flocculation. Further, the water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped on No.2 filter paper, to show bleeding of the dye.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06648954B2
Source datasetuspto-grants-2003_11
ORD IDord-a93018f0c5a346c381a6a0cd5b462802
Source noteuspto-grants-2003_11