Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 5,12-Dihydro-2,9-dimethylquino(2,3-b)acridine-7,14-dione | HCID 70423 | — |
| Reactant | HCID 178427422 | HCID 178427422 | — |
| Solvent | Water | HCID 962 | — |
| Product | Quinacridone | HCID 13976 | — |
Reaction Steps
20 g of C.I. pigment red 122 having an average primary particle diameter of 90 nm (in which the content of metal ion having a valence of at least 2 was 450 ppm), 4 g of a commercially available dye C.I. acid red 249 and 110 g of deionized water were mixed, a 1% by weight sodium hydroxide aqueous solution was added so as to adjust the pH of a mixture liquid to 9.0, and the mixture liquid was dispersed with a paint shaker in the presence of zirconia beads as media for approximately 5 hours, to obtain a water-based pigment dispersion. The obtained water-based pigment dispersion had a high viscosity and caused flocculation. Further, the water-based pigment dispersion was diluted so as to have a concentration of 3% by weight, and the diluted water-based pigment dispersion was dropped on No.2 filter paper, to show bleeding of the dye.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06648954B2 |
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| Source dataset | uspto-grants-2003_11 |
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| ORD ID | ord-3a1ff11946e644808af56a9d89ffe3cd |
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| Source note | uspto-grants-2003_11 |
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