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HRID480005

反应详情

EQUATION

反应方程式

HRID 480005 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：O=C(O)CC(CC(=O)O)c1ccccc1
HCID77823

3-Phenylglutaric acid

C11H12O4

PRODUCTS

生成物

1
结构：O=C1CC(c2ccccc2)CC(=O)O1
HCID297882

3-Phenylglutaric anhydride

C11H10O3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

10 mmol of 3-phenylglutaric acid and 30 mmol of acetic anhydride are heated under reflux until they have dissolved completely. After cooling, 3 ml of diethyl ether are added and the precipitate is filtered off and washed with diethyl ether. This gives 3-phenylglutaric anhydride.

WORKUP

后处理

  1. temperatureunder reflux until they
  2. dissolutionhave dissolved completely
  3. temperatureAfter cooling
  4. filtrationthe precipitate is filtered off
  5. washwashed with diethyl ether