HCID 15521042, compound → HCID 18768633, compound

HRID 480034Notes

Reaction equation

HRID 480034 reaction equation
[Cl:1]C1C=C(Cl)C=CC=1OCCCN1CC=CCC1.[Cl:19][C:20]1[C:35]([Cl:36])=[C:34]([Cl:37])[CH:33]=[CH:32][C:21]=1[O:22][CH2:23][CH2:24][CH2:25]N1CC=CCC1>>[Cl:37][C:34]1[CH:33]=[CH:32][C:21]([O:22][CH2:23][CH2:24][CH2:25][Cl:1])=[C:20]([Cl:19])[C:35]=1[Cl:36]

Participants

3

Reactant 2

HCID 15521042HCID 15521042, compoundHCID 18768639HCID 18768639, compound

Product 1

HCID 18768633HCID 18768633, compound

Procedure

IR (CHCl3); 3022, 2968, 2884, 1577, 1448, 1422, 1386, 1285, 1256, 1220; NMR (CDCl3) δ (300 MHz); 2.290 (quint., J=6 Hz, 2H); 3.798 (t, J=6 Hz, 2H); 4.180 (t, J=6 Hz, 2H); 6.824 (d, J=9 Hz, 1H); 7.322 (d, J=9 Hz, 1H). (2) Preparation of 3g; 1-[3-(2,3,4-Trichloro-phenoxy)-propyl]-1,2,3,6-tetrahydro-pyridine

Sources & evidence

ORD record
ord-4a2a5b7744754139b67944c8c26547e1
Source dataset
uspto-grants-2003_11
Patent number
US06649623B1

Reaction notes

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