HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acetylhydroquinone → HCID 57143294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acetylhydroquinone | HCID 10279 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Epibromohydrin | HCID 18430 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 57143294 | HCID 57143294 | — |
Reaction Steps
A solution containing 3.00 g (0.020 mole) of 2,5-dihydroxyacetophenone, 3.37 ml (0.040 mole) of epibromhydrine and 5.06 g (0.040 mole) of K2CO3 in 30 ml of acetone are heated for 8 hours under reflux. The solvent is evaporated off, 20 ml of a saturated solution of NaH2PO4 and 120 ml of water are added, and an extraction carried out with ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06649627B1 |
| Source dataset | uspto-grants-2003_11 |
| ORD ID | ord-699c6643bb1f4eef8b15b6271e1fdc52 |
| Source note | uspto-grants-2003_11 |