Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 3,5-Dichlorobenzaldehyde | HCID 35746 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 3,5-Dichlorocinnamic acid | HCID 176504 | 61.8% |
Reaction Steps
A mixture of 3,5-dichlorobenzaldehyde (15.0 g, 85.7 mmol), malonic acid (12.5 g, 120.2 mmol), and piperidine (5 mL) was heated at 100° C. for 2 h and at 150° C. for 1 h. The reaction was poured onto 3N HCl (200 mL) and the precipitate was removed via filtration. The product was purified by recrystallization (100 mL hot EtOH) to afford 3-(3,5-dichlorophenyl)-acrylic acid (11.5 g). 1H NMR (250 MHz, DMSO-d6) δ 12.6 (bs, 1H), 7.83 (m, 2H), 7.64-7.51 (m, 2H), 6,72 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06649657B2 |
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| Source dataset | uspto-grants-2003_11 |
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| ORD ID | ord-0baac6ca50e342d2a367d68d878c432b |
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| Source note | uspto-grants-2003_11 |
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